- CasNo18063-03-1
- Purity99%
Location:Home > Pharmaceutical
Perfect Factory Offer Excellent quality 2,6-Difluorobenzamide 18063-03-1 with Safe Shipping
- Molecular Formula:C7H5F2NO
- Molecular Weight:157.12
- Appearance/Colour:white powder
- Vapor Pressure:0.622mmHg at 25°C
- Melting Point:145-148 °C(lit.)
- Refractive Index:1,508
- Boiling Point:187.7 °C at 760 mmHg
- PKA:14.54±0.50(Predicted)
- Flash Point:67.3 °C
- PSA：43.09000
- Density:1.348 g/cm3
- LogP:1.76400
2,6-Difluorobenzamide(Cas 18063-03-1) Usage
InChI:InChI=1/C7H5F2NO/c8-4-2-1-3-5(9)6(4)7(10)11/h1-3H,(H2,10,11)
18063-03-1 Relevant articles
SYNTHESIS OF VARIOUS AROMATIC AMIDE DERIVATIVES USING NITRILE HYDRATASE OF RHODOCOCCUS RHODOCHOROUS J1
Mauger, Jacques,Nagasawa, Toru,Yamada, Hideaki
, p. 1347 - 1354 (1989)
Nitrile hydratase, that is produced abun...
Preparation method of 2,6-difluorobenzamide
-
Paragraph 0074; 0080-0081; 0082-0085; 0086-0090; 0091-0094, (2021/05/29)
The invention provides a preparation met...
Design, synthesis, and bioactivities of novel pyridazinone derivatives containing 2-phenylthiazole or oxazole skeletons
Dang, Mingming,Liu, Minhua,Huang, Lu,Ou, Xiaoming,Long, Chuyun,Liu, Xingping,Ren, Yeguo,Zhang, Ping,Huang, Mingzhi,Liu, Aiping
, p. 4088 - 4098 (2020/10/02)
A series of novel pyridazinone derivativ...
Synthesis method of insecticide teflubenzuron and intermediate 2,6-difluorobenzamide of insecticide teflubenzuron
-
Paragraph 0056; 0060; 0064; 0068; 0072; 0076, (2020/12/10)
The invention discloses a synthesis meth...
Ti-superoxide catalyzed oxidative amidation of aldehydes with saccharin as nitrogen source: Synthesis of primary amides
Kamble, Rohit B.,Mane, Kishor D.,Rupanawar, Bapurao D.,Korekar, Pranjal,Sudalai,Suryavanshi, Gurunath
, p. 724 - 728 (2020/01/23)
A new heterogeneous catalytic system (Ti...
18063-03-1 Process route
-
-
18063-02-0
2,6-difluorobenzoylchloride
-
-
18063-03-1
2,6-difluorobenzamide
Conditions
| Conditions | Yield |
|---|---|
|
With
ammonia;
|
|
|
With
ammonium hydroxide;
Yield given;
|
|
|
With
ammonia;
|
|
|
With
ammonia;
|
|
|
With
ammonium hydroxide;
at 0 - 10 ℃;
for 1h;
|
|
|
With
ammonium hydroxide;
In
dichloromethane;
at 0 - 20 ℃;
for 3.5h;
|
|
|
With
ammonium hydroxide;
In
tetrahydrofuran;
at 0 - 20 ℃;
|
|
|
With
ammonium hydroxide;
In
toluene;
at 0 - 20 ℃;
|
-
-
1897-52-5
2,6 difluorobenzonitrile
-
-
18063-03-1
2,6-difluorobenzamide
Conditions
| Conditions | Yield |
|---|---|
|
With
water;
nitrile hydratase from Rhodococcus rhodochrous J1;
at 25 ℃;
for 22h;
KH2PO4-K2HPO4 puffer pH=8.0;
|
100% |
|
With
dihydrogen peroxide; sodium hydroxide;
at 50 ℃;
for 5h;
Temperature;
|
91.2% |
|
With
sulfuric acid;
at 70 ℃;
for 4h;
|
90% |
|
With
dihydrogen peroxide;
at 30 ℃;
for 6h;
|
90.2% |
|
With
water;
|
78% |
|
With
manganese(IV) oxide; silica gel;
In
chlorobenzene;
for 5h;
Heating;
|
41% |
|
With
sulfuric acid;
In
ice-water; water;
|
91.0 g (80.6%) |
|
With
dihydrogen peroxide; potassium carbonate;
In
dimethyl sulfoxide;
at 0 - 25 ℃;
|
|
|
With
nitrile hydratase from Rhodopseudomonas palustris CGA009;
In
dimethyl sulfoxide;
at 30 ℃;
for 17h;
pH=7;
chemoselective reaction;
aq. phosphate buffer;
|
18063-03-1 Upstream products
-
18063-02-0
2,6-difluorobenzoylchloride
-
1897-52-5
2,6 difluorobenzonitrile
-
19064-16-5
2,6-difluoro-benzaldehyde oxime
-
385-00-2
2,6-difluorobenzoic acid
18063-03-1 Downstream products
-
60731-73-9
2,6-difluorobenzoyl isocyanate
-
35367-38-5
1-(4-chlorophenyl)-3-(2,6-difluorobenzoyl)urea
-
130535-64-7
N-(2,6-Difluorobenzoyl)phthalimide
-
116800-81-8
1-(2,6-Difluoro-benzoyl)-3-(3-fluoro-phenyl)-urea
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